;z_sc_cosy ;avance-version ;homonuclear strong coupling 2D correlation with Z-filter la Keeler ; ;B. Luy, ;Adiabatic z-filtered J-spectroscopy for absorptive homonuclear decoupled spectra ;J. Magn. Reson. ; #include #include ;######### AVANCE III ########### "acqt0=0" "in0=inf1/2" ;###################################### "p2=p1*2" "d0=3u" 1 ze 2 d1 3 p1 ph1 d0 d0 p2 ph2 p1 ph3 3u pl0:f1 50u UNBLKGRAD 300u gron0 p11:sp1:f1 ph4 100u groff 4u BLKGRAD 4u pl1:f1 p1 ph4 go=2 ph31 d1 mc #0 to 2 F1PH(ip3, id0) exit ph1=0 ph2=0 2 ph3=2 ph4=0 ph31=0 ;pl1 : f1 channel - power level for pulse (default) ;p1 : f1 channel - 90 degree high power pulse ;p2 : f1 channel - 180 degree high power pulse ;p11 : f1 channel - Keeler z-filter pulse CHIRP ;sp1 : f1 channel - Keeler z-filter pulse CHIRP ;gp0 : gradient for Keeler z-filter ;d0 : incremented delay (2D) [3 usec] ;d1 : relaxation delay; 1-5 * T1 ;in0: 1/(2 * w), w = max. width of multiplet ;nd0: 2 ;NS: 4 * n ;DS: 16 ;td1: number of experiments ;MC2: ;see Thrippleton, Keeler, Angew. Chem. Int. Ed. 2003 ;and Keeler website for details regarding z-filter